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Nguoàn taøi chính do toå chöùc  Löông - Noâng theá  giôùi, thoâng qua Hieäp Hoäi chaên nuoâi, uûng hoä veà vieäc chuaån bò nhöõng taøi lieäu söû duïng nhöõng chaát thaûi taùi sinh..

Taùc giaû thaønh thaät caûm ôn nhöõng yù kieán  ñoùng goùp veà nhöõng thieáu soùt.

Trôû veà muïc luïc

University of Tropical Agriculture

Thu Duc, Ho Chi Minh City

Vietnam

 

 

 

 

 

 

 

 

 

 

 

 

Laboratory   Manual

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

J. :Ly and Nguyen Van Lai

UTA Ecolaboratory

 

1997

 

 

 

 

 

 

 

 

 

 

Preface

 

 

These instruction are for the use in the LABORATORY and should be seen as Manual for every - day work. The equipments and technique use in this manual very simple and easy to use. Supply for any one who want to research.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

                                                           

 

Table of contents

 

 

                                 Dry matter

                                 HCN

                                 Amoniac

                                 Nitrogen

                                 NDF

                                 ASH

                                 Disolved oxygen

                                 In vitro ileal digestibility

                                 In vitro gas production

                                 pH

                                 Wash value

                                 Water soluble solids

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Preparation of  the sample

 

The sample preparation serves several purpose

 

1/ To get the sample ready for grinding

2/ to get it in the proper physical state standardized particel size

3/ To get the sample suitable for storage

 

It is a big advantage to pre - dry all samples because the grinding will be much easier and the samples will not deteriorate during storage.

 

The first step of the sample preparation is the mixing of the whole sample brought to the laboratory. This includes in some cases chopping. Take care not to get any separation of the fine particels during this mixing step.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

                  

 

 

 

 

 

 

Determination of dry matter (DM)

 

The principle of the method is that, by heating a certain sample, it is possible to eliminate all its water content, and then dry material is obtained. This technique necessitates a balance and a heating device, usually an oven.

Instructions

 

1/ Weight a dry and clean container.

2/ Add the original, fresh sample to the container, and weight both of them together.  This

    operation is made at least in duplicates of the same sample.

 

3/ Dry the sample to constant weight, which implies that all the water has been eliminated.

 

4/ Weight the dry sample in the container.

 

 

 

Calculations

 

                            % DM = (DS/OS) x 100

 

   Taking into account the weight of the container (C), then

   OS = Weight of the original sample, and (OS + C)- C = OS

   DS = Weight of the dry sample, and (DS + C) - C = DS

 

Example

 

The weigh of a sample of fresh leaves plus a container was 15.12g and 13.40g in the fresh (original) and dry state, whereas the weight of the container was 12.88 g. Then :

 

    OS = 15.12 - 12.88 = 2.24 g

    DS = 13.40 - 12.88 = 0.52 g

 

Therefore, % DM = (0.52/ 2,24) x 100 - 23.21 %

 

The DM content from a duplicate of the same sample was 22.8%. Then the average DM content of the sample of leaves was.

 

Average % DM = (23.21 + 22.87)/2 = 23.04.

 

 

 

 

 

 

 

 

 

 

 

Determination of HCN

 

Principle :

Procedure :

Weigh of the samples ( fresh leaf about 20 grams, dry leaf about 5 grams)   and then put in to flask kieldalh add 250 - 300 ml distill water and add  8 ml Chloroform  after that boiling them.

 

Put 8 ml potassium hydroxyt 0.1 N into a 250 ml E - flask and place it on the upper shelf with receive tube dipped in the potassium. When there is 100 ml in the E - flask it OK. 

 

Titration with Nitrate silver 0.1 N the colour from white in to chase white colour

 

Calculation :

                                        V * 0.005204

                 % HCN =    ----------------------    * 100

                                             Weight

 

                             V   : ml silver nitrate titration

 

                  0.005204 : 1 ml silver nitrate equivalent  0.005204 g HCN

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of Amoniac

 

Principle :

Procedure :

- Weight of the samples and then put in to the kieldalh

     add about 5 g Oxyt magie

     add 300 ml distill water after that boiling them.

 

- Using 250 ml triangle bottle  add 50 ml boric acid 4% collect amoniac until 200 - 250 ml 

   and then titration with sulfuric acid 0.1 N. The colour from white in to initial pink

 

Calculation :

                                                V * 0.0017

                   % Amoniac =    ----------------   * 100

                                                     Weight

 

 

                    V : ml acid titration

                     0.0017 : constant 1 ml acid equivalent 0.0017 g  amoniac

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of Nitrogen

 

Prepare chemical

 

- Salt mixture : K2SO4 : CuSO4. 5H2O in to 10 : 1 proportion

  Take 1000g K2SO4 and mix well with 100g CuSO4.5H2O

 

- Sulphuric acid for digestion : Concentrated, ind. Grade is enough

 

- Sodium hydroxide : 40% NaOH in tap water = 10 N

  Dissolve 2kg NaOH in tap water and make up to 5 litter

 

- Mix indication : Methylenblue and Methyl red

   Dissolve 0.12g Methylen blue in 100 ml Ethanol

   Dissolve 0.270g Methyl red in 200 ml Ethanol

   Mix the two!

 

*Boric acid + indicator

  2% boric acid in water + mix indicator

  Dissolve 100 g of boric acid in water and make up to 5 litter.  Add 25 ml of mixed indicator.

 

* Sulphuric acid for titration 0.1 N

   Prepare a 1,00 N (0.5 M) H2SO4 from aspulle if possible.

   Dilute it 10 times. Take 100 ml and make up to 1000 ml

 

 

Principles

 

Procedure

Digestion

 

Weigh accurately samples and put samples in to kieldald  flask add 10 - 15 g of this salt mixture and add 25 ml acid sulphuric concentration and then put the flask on the heaters  and boiling them.

Digest until the colour has turned green it Ok

Allow the flask to cool down for at least 30 min

 

Add 250 ml of distill water

 

Distillation

 

Put 50 ml of boric acid + indicator solution in to a 250 - 300 ml E - flask and place it on the upper shelf with the receiver tube dipped in the acid

Pour careful 90 - 100 ml of NaOH 40% in the flask

connect the flask to the distiller and then shake it carefully. This has to be done as quickly as possible to avoid lossed of nitrogen

When there is 150 ml in the E-flask, lift it down to the lower shelf, continue the distillation until there is 175 ml in the E-flask

Wait for 5 - 10 minute so the last distillate can come down into the E-flask

Titration and calculation

Titration with 0.1 N H2SO4 until the colour is between green and purle

correct the titer with the blank - value

Two blanks should be run every time a new preparation of boric acid is used and also when you start using a new bulk of any of the chemicals.

 

Calculation

 

                              (Titer - blank x 0.875)

          % CP =     ----------------------------

                                Sample weight (g)

 

 

                                    (Titer - blank x 0.14)

          % Nitrogen =   --------------------------

                                      Sample weight (g)

 

                                0.1 x 0.014 x 6.25 x 100

           * 0.875 =   -------------------------------

                                                                                    1000

 

           * 0.1    = The strength of the acid for titration

           * 14     =  Formula weight for nitrogen

           * 6.25  = Factor to transfer from nitrogen to protein on most feed samples

           * 1000 = Conversion from liters to milli - liters

           * 100   = To get %

 

Note : Always use protectives like lab, coats, gloves and spectacles when working with 

           strong acids and alkalines.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of NDF

 

Prepare chemicals for NDF

 

Bottle 1 : 150 g sodium dodecyl sulfate + 50 ml Tri - ethylenglycol + 2 litter water

Bottle 2 : 93.05g EDTA + 34.05g sodium tetraborate + 1 litter water

Bottle 3 : 22.8g Disodium hydrogen phosphate + 1 litter water gently boiling and cool down

Bottle 4 = put 2 and 3 into 1 adiust until 5 litters and correct pH 6.9 - 7.0 it OK

 

Principle

 

Procedure

Weigh accurate 1 - 1.5g of the grinded sample into a beaker (600ml) or flask. Add 100 ml of NDF - solution and 2 ml of decalin.

Heat to boil and reflux for 60 minute

Place a previously tared glassfillter - crucible on the filtermaniflold. Transfer contents of beaker to the crucible while using low vacuum from the beginning. Rinse beaker with hot water and also the residue in the crucible with hit water. Rinse finally twice with acetone. Dry crucible at 105oC over night. Weigh out after cooling down in a desiccator. Ash at 500oC for 2 - 3 hours. Cool down in desiccator and weigh again.

 

                                          OS - DR

               % WL (DM) =  -------------- x 100

                                               OS

 

                                                          Weigh after drying - Tare weight

                   NDF (INCL ASH) % =   ------------------------------------------ x 100

                                                                        Sample weight

 

                                                        Weigh after drying - weigh after ASH

             NDF (EXCL ASH) % =     -------------------------------------------------- x 100

                                                                         Sample weight

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of  total  ASH

 

Weigh accurately ( 1 mg) 1 - 5 grams of sample into a tare porcelain crucible. Ash the material until greyish ash results in an electric furnace at 550 oC - 600 oC . The time it takes depends on the sample and the furnace, normally 3 - 4 hours. Cool the crucible and its contents in a desiccator and weigh. If the ash is not greyish you could treat it with hot water, filter through, ashfree filterpaper, wash with hot water and transfer the filterpaper to a crucible and ash again for 5 - 10 min, then cool in a desiccator and weigh

 

Calculation

                                           Weight of sample after ashing

                       ASH % =    ------------------------------------------- x 100

                                           Weight of sample before ashing

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of dissolved oxygen

 

The oxygen which is dissolved in water is determined by a portable disolved oxygen meter (DO meter) from Hanna instruments (HI 8543). The principle of the determination is based on polarography. The DO meter has a disolved oxygen probe consisting of a membrane covering the polarographic sensor and a built-in thermistor for temparature measurements and compensation. Dissolved oxygen can be estimated in the range of 0.0 to 19.9 mg/l with a resolution of 0.1mg/l and an accuracy of 0.2 mg/l.

 

Instructions

 

1/ Connect the DOmeter with the DO probe and switch on. Wait about 10 minutes to ensure

    the probe has been polarized.

 

2/ Prepare the electrolyte solution by adding 15 to 20 drops of HI 7041 solution into 20 ml of

    distilled water.

 

3/ Wet the sensor by soaking the bottom of the probe in the dilute electrolyte solution for 5

    minutes.

 

This is done by unscrewing the protective red and black plastic cap. Ensure the o-ring is properly placed inside the membrane. Rinse the membrane cap with electrolyte while shaking it gently. Refill with fresh electrolyte. Gently tap the sides of the membrane with the finger tip to ensure that no air bubbles remain. To avoid damage, do no tap the membrane directly on the bottom. With the sensor facing down, firmly screw the membrane cap clock -wise to the end of the threads. Some electrolyte will overflow.

 

4/ For slope calibration, rinse the probe throughly (particularly after the zero calibration) with

   some water and blot dry in a manner as not to damage the membrane (use cloth or soft  

   paper). Place the probe in vertical position in air. Wait a few minutes until the 

   measurement stabilizes.

   Press and hold the red button between the two calibration screws. The decimal point should     disappear from the display. Using a small screwdriver, turn the slope trimmer until the  

   display reads 100. Release the red button and the display will show the saturation value at

   that ambient temperature. Saturation value is the maximum dissolvable oxygen value in a

   liquid at that temperature.

 

5/ Dissolved oxygen is determined in the samples after slope calibration. All the 

   measurements  are referred to sea level and zero salinity..

 

 

 

 

 

 

 

 

 

In vitro ileal digestibility of dry matter (DM), N and

               organic matter (OM) in pigs.

 

Principle

The in vitro estimation of ileal digestibility permits the evaluation of the quality of feeds, specially N and amino acids for pigs. It has been well established the straight correlation which does exits between in vitro ileal and in vitro (pepsin/ pancreatin), and in turn, the interdependence between in vitro ileal N digestibility and performance traits of economic importance in pigs.

 

The methods herein described is that proposed by Dierick et al (1985) fully developed in tropical non conventional feeds at the swine Research Institute at Havana by the research team of Ly (see for example, Dominguez et al 1996).

 

Procedure

 

1/ Weight an amount of dry and ground sample containing 150 mg of protein (N x 6.25) and

    put it into a 100 ml erlenmeyer flask. Add 20 ml of a pepsin solution ( 1mg enzyme/`ml

    HCL 0.075 N) plus a drop of timerosal.

 

2/ Incubate the sample in a water bath at 37oC (preferably 80 strockes per minute) during 4

    hours.

 

3/ Neutralize until pH = 7.5 with NaOH (or KOH) 0.2N ( about 7.5 ml).

 

4/ Add 20 ml of a solution of 15% pancreatin in a phosphate buffer. The phosphate buffer

    can be prepare by mixing 10 of a solution of 31.50g KH2PO4.3H2O/ L and 90 ml of

    another solution of 45.6g K2HPO4/ L. The solution is adjusted to pH = 7.5 and made up to

    a L with distilled water. Repeat the incubation in a water bath at 37oC as in 2.

 

5/ Add a solution of sodium tungstate (5%) to precipitate the undigested protein.

6/ Transfer the solution quantitatively to a 120 ml centrifuging tube and centrifugue the

     sample during 10 minutes at 1250 rpm. As alternative, filter quantitatively, in a previously

     weighed filter paper.

 

7/ Dry to constant weight to determine the dry insoluble residue

8/ Determine the ash content in other dry insoluble residue to calculate the insoluble organic

    matter.

9/ Determine the N content by the Kjeldhal procedure in another dry insoluble residue.

 

Calculation

                                                   OS - DR

                     % IVDDM =      --------------- x 100

                                                       OS

 

      Where :

                   * OS = Weight of the original sample, in dry basis

                   * DR = Weight of the dry residue

 

When the in vitro digestibility of organic matter (IVDOM) or in vitro digestibility of N (IVDM) is to be estimated, calculate by the same procedure for example, the IVDN should be calculated by the following equation.

 

 

                                               NOS -N DR

                     % IVDN =      -------------------  x 100

                                                     N OS

 

        Where :

                      * NOS = mg of N in the original sample

                      * NDR = mg of in the dry residue.

 

References

 

Dierick, N, Vervaeke, I., Decuypere, J. and Henderickx, H. 1985. Protein digestion in pig measured in vitro and in vitro. In : Proc, 3rd Int. Seminar Dig. Physiol. Pig (A. Just, H. Jogensen and J. A. Fernandez, ed.) Kobenhavn p 329 - 332.

 

Dominguez, P. L., Molinet, Y. and Ly, J. 1997. Ileal and in vitro digestibility in the pig of three floating aquatic macrophytes. Livest. Res. Rural Devel. 8(4) : 37 - 44.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of the in vitro gas production.

 

The in vitro gas production (IVDP) technique measures the evolution of gases (methane and carbon dioxyde) which are produced as end products of fermentation in the rumen. Production of carbon dioxyde is partly from the fermentation and partly as result of formation of short chain fatty acids which expels carbon dioxyde from the bicarbonate buffer solution.

 

The method is important for feed evaluation, particularly to predict animal performance such as feed digestibility and intake in the ruminant. It has the advantage of the in vitro technique a great number of samples can be evaluate at the same time, it is time saving and cheaper than those methods requiring the use of animals, thus becoming expensives by feed cost.

 

The IVGP technique provides a great advantage in that the fermentation take place in a glass syringe which allow for several measurements to be made in the same by measuring the gas volume at different intervals of time. This means that not only the possible extent of fermentation can be measured.

 

The procedure herein described is that of Menke and Steingass (1988)

 

Instroduction

 

1/ All substrates should e milled using a 1mm screen. Weigh 200 mg substrate into each

    (numbered) syringe and record actual weight. Include a blank (for example. Rumen fluid/

    buffer mixture on its own) at the beginning, in the middle of the set, and at the end. A

    sample of hay can be milled and used as a control by including a syringe with the hay at

    the beginning and the end of each rum. Samples should be done in duplicate or triplicate.

    After the weighings are completed, grease the plungers with vaseline, and place in

    incubator at 38oC. This is normally done the day before the run.

 

2/ Measure distilled water, buffer solution, macromineral solution, micromineral solution

    and resazurin solution into a round, flat bottomed, flask - warm to 38oC. Then add

    reducing solution of sodium sulphide. Place it in a small water bath on magnetic stirrer,

    put magnet into flask and gently bubble carbon dioxyde through the solution until the blue

    color turn to pink, then clear. This means the buffer solution is now reduced. Raise the

    carbon dioxyde tube so that it will be above the level of the buffer/ rumen fluid mixture,

    but providing a stream of carbon dioxyde into the flask throughout the dispensing

    procedure. The pH of buffer should be 7 - 7.3.

 

3/ Collect rumen fluid from the donnor animal, strain through gauze into a warm beaker, the

    final ratio of rumen buffer fluid should be 1:2 Mix rumen fluid in beaker and transfer to

    flask with buffer solution. Make sure the magnet is mixing properly during the whole

    process of dispensing the buffer/ rumen fluid mixture into the syringes. Add 30 ml to each

    syring using the dispenser (do 2 - 3 times 30 ml amounts into a beaker at the beginning to

    be sure the dispenser is properly charger). Fill the syringe, then open the clip and gently

    push the plunger of the syringe so that all the gas is removed. Record the level in each

    syringe and place it in the water bath.

 

Times of reading can be chosen to suit the type of substrate in the syringes. For forages 3 hours, 6 hours, 12 hours, 24 hours, 48 hours, 72 hours and 96 hours are suitable but for concentrate type substrate it may be necessary to take more reading in the first 24 hours. It is advisable to gently mix each syringe     2 - 3 the lectures made at 24 hours and 48 hours.

 

Gas production is estimated in ml/ 0.2 g of sample per 48 hours.

Preparation of solution

 

1/ Macromineral solution.

                                           Na2HPO4            5.7 g

                                           KH2PO4              6.2 g

                                           MgSO4. 7H2O     0.6 g

    Make up to one liter with distilled water

 

2/ Buffer solution

                                NaHCO3         35 g

                                (NH4)HCO3      4 g

 

    Make up to one liter with distilled water

 

3/ Micromineral solution

 

                                        CaCL2. 2H2O         13.2 g

                                        MnCL2. 4H2O        10.0 g

                                        CoCL2. 6H2O           1.0 g

                                         FeCL2. 6H2O           0.8 g

 

    Make up to 100 ml with distilled water

 

4/ Reducing solution

                                   NaOH 1N                2   ml

                                   Distilled water      47.5 ml

                                   Na2.7H2O           0.285 g

 

5/ Resazurin solution

                                 Resazurin 0.100 g

   Make up to 100 ml with distilled water

 

6/ Preparation of the buffer solution

 

    Distilled water                                      474 ml

    Macromineral solution (number 1)      237 ml

    Buffer solution   (number 2)                 237 ml

    Micromineral   (number 3 )                 0.12 ml

    Resazurin solution (number 5)             1.22 ml

 

   Warm to 38oC, then add reducing solution (number 4), prepared fresh for each run.

 

 

 

 

 

Determination of pH

 

The pH value in different types of samples is determined by a portable digital pHmeter. The principle of the determination is based on potentiometry. Thee pHmeter has a pH combination electrode and pH values can be estimated in the range of 0.00 to 14.00 with a resolution of 0.01 and accuracy of 0.01.

Instructions

 

1/ Connect the pHmeter with the pH electrode and switch. Set the mode switch to thr pH

    position. This will activate the liquid cristal display. Condition the electrode in buffer 7.00

    until the display is fully stable (about 30 minutes). Give a stirring action to the electrode

    each time it is placed in a new solution.

 

2/ Adjust the calibration control to make the display read the value of buffer 7.00. Rinse the

    electrode with distilled water and blot dry.

 

3/ Inmerse the electrode in buffer 4.00. When the display is stable (30 seconds), adjust the

    slope control to make the display read the value of buffer 4.00. The pH value are 6.99 and

    4.01 for buffer 7.00 and 4.00 respectively at 30oC. Error may be minimum in the case that

    pH value are not adjust to the temperature of the solution to be tested.

 

   The apparatus is now calibration to read samples with pH 0 - 14.

 

4/ Rinse the electrode with distill water, blot dry and inmerse in the saple. The sample must

    be homogenous. When the display is stable (30 seconds), it will read the pH of the sample

    Repeat this step for continued samples. Periodically check calibration, at least one per day.

 

5/ When all samples are completed, keep the electrode inmerse in distilled water. The

    electrode shall never be kept dry, otherwise electrode damage shall be irreversible.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of the wash value

 

Washing losses or a wash value of a sample are considered to be the amount of water soluble substances readily utilizable by the animal. This technique was first applied to ruminant studies concerning the digestibility of roughages.  It now has been suggested to be directly related to the cell contents (100 - NDF) of a sample, which in turn, could be of application in non ruminant nutrition studies too.

 

The method herein described it that proposed by Ly and Preston (1997) which studies some detail of the analytical technique, not taken into consideration previously. This technique requires a balance, an oven and a comercial semiautomatic washing machine. On the other hand, it is necessary to use nylon bags of 50 x 50 mm. This bag are made of nylon filter cloth with a pore size of 45 to 55 micrometers, and are available from some catalogue list.

 

Instructions

 

1/ Weight a dry and clean bag

 

2/ Add to the bag, very carefully, 1 g f air - dried sample or 5 g of fresh sample. Weight again

    this operation is made at least in triplicate of the same sample. The mouth of the bag must

    be tightly close, such as to avoid losses during washing. This procedure can be afford by a

    rubber band.

 

3/ Wash the bag in a comercial, semiautomatic washing macbine of 15 min - cycle, during 90

    min, discarding the water every two cycle. Use tap water at room temperature. The ratio of

    water per bag is of 3 litters.

 

4/ After washing, let the bag to drain and dry it in an oven to constant weight

 

5/ Determine the wash value taking into account the original dry matter of the sample.

 

6/ The sample is followed for determining the wash value of nitrogen in the sample. In this

     opportunity, the N content in the original and in the washed sample should be used for

     calculations.

 

Calculations

                                                  OS - DR

                       % WL (DM) =  -------------- x 100

                                                       OS

 

Where OS is the weight in g of the original sample, in dry basis, and DR is the weight in g of the dry residue.

 

If it is desire to determine the wash value of N in the sample, then the calculation will be as follows

 

                                                 NS - NR

                         % WL (N) =  -------------- x 100

                                                      NS

 

Where NS and NR in the nitrogen content determined in the original sample and in the residue obtain after washing. The nitrogen content is usually expressed in percent in dry basis, in both cases.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Determination of water soluble solids

 

Water soluble solids (WSS) are estimated by refractometry, taking into account that a straight interdependence exists between brix and refractive indices in certains solutions. A hand refractometer (Fisher Scientific, catalogue No. 13 - 946 - 60A) will be used for WSS determination in leaves and sugar cane juice. The measuring range of the instrument is 0 - 32% (accuracy, 0.2%)

 

Calibration procedure

 

1/ Keep distilled water and instrument at room temperature (20oC) for 1 hours.

 

2/ Open the prism cover and put one or two drops of distilled water on the prism. Close the

    prism gently.

 

3/ Direct the prism towards a light source and look at the scale through the eyepiece.

 

4/ Rotate the view control to a clean image of the scale. Real the scale. It the scale is correct,

    the boundary line meets with “0" position. No calibration is needed. IF the boundary line is

    out of “0" position, calibration the boundary line to indicate “0" position by turning the

    calibration screw with a screwdriver.

 

5/ Calibration is completed wipe off the distilled water from the prism with a soft clean cloth

    or tissue paper.

 

Instructions.

 

1/ Open the prism cover and put one or two drops of the sample in the prism.

2/ Close the prism cover gently

3/ The sample volume must cover the prism surface entirely

4/ Direct the prism towards a light source and look at the scale through the eyepiece

5/ Rotate the view control to focus a clean image of the scale. Real the scale where the 

    boundary line interrupts it.

6/ After every measurement, wipe the sample from the prism with a soft cloth of tissue paper 

    and water. Keep the prism clean and dry to get the correct reading.

7/ Calculate WSS content (Brix %) from the determined refractive indice (nD), see table 1

 

Table 1 : Brix (%) vs refractive index (nD)

 

Brix (%) Refractive indices (nD)               Brix (%)      Refractive indices (nD)

0                                                                                                          1.33299                                   17                    1.35890

1                                                                                                          1.33423                                   18                    1.36053

2                                                                                                          1.33588                                   19                    1.36218

3                                                                                                          1.33733                                   20                    1.36384

4                                                                                                          1.33880                                   21                    1.36551

5                                                                                                          1.34027                                   22                    1.36719

6                                                                                                          1.34176                                   23                    1.36888

7                                                                                                          1.34027                                   24                    1.37059

8                                                                                                          1.34477                                   25                    1.3723

9                                                                                                          1.34629                                   26                    1.3740

10                                                                                                        1.34783                                   27                    1.3758

11                                                                                                        1.34937                                   28                    1.3775

12                                                                                                        1.35093                                   29                    1.3793

13                                                                                                        1.35250                                   30                    1.3811

14                                                                                                        1.35408                                   31                    1.3829

15                                                                                                        1.35567                                   32                    1.3847

The hand refractometer is designed to be used at 20oC, and when used above 20oC, the reading value (brix %) have to be correcting referring to table 2 by adding the following value.

 

 

 

 

Table 2 : Temperature compensation table

 

Reading (Brix %)

 

Temperature (oC)             0            5            10            5            20            25            30            35

25                                                                                                                                            0.33     0.35     0.36     0.37     0.38     0.38     0.39     0.39

26                                                                                                                                            0.40     0.42     0.43     0.44     0.45     0.46     0.47     0.47

27                                                                                                                                            0.48     0.50     0.52     0.53     0.54     0.55     0.55     0.55

28                                                                                                                                            0.56     0.57     0.60     0.61     0.62     0.63     0.63     0.63

29                                                                                                                                            0.64     0.66     0.68     0.69     0.72     0.72     0.72     0.72

30                                                                                                                                            0.72     0.74     0.77     0.78     0.79     0.80     0.80     0.81